Date of Award

2026

Document Type

Open Access Master's Thesis

Degree Name

Master of Science in Materials Science and Engineering (MS)

Administrative Home Department

Department of Materials Science and Engineering

Advisor 1

Sriram Vijayan

Committee Member 1

Walter Milligan

Committee Member 2

Yongmei Jin

Committee Member 3

Steven Kampe

Committee Member 4

Daniel Segiun

Abstract

Laser Powder Bed Fusion (LPBF) enables fabrication of metallic parts with intricate geometries, low ‘buy to fly’ ratio, and reduced tooling in small batches. The non equilibrium nature of the LPBF process results in steep thermal gradients, rapid solidification and rapidly fluctuating thermal cycles that promote the formation of high-temperature metastable phases, including δ-ferrite and austenite in alloys like 17-4 Precipitation Hardened (PH) Stainless Steel, which typically consists of a martensitic microstructure in the cast and wrought form. These metastable microstructures formed in 17-4PH SS LPBF parts result in mechanical properties that are vastly different from their conventional processed counterparts, presenting a major barrier to industrial adoption. These challenges reveal a major gap in our understanding of the physical metallurgy of LPBF parts. Therefore, a thorough and systematic assessment of process-structure-property relationships is required, to ensure consistent microstructural control, predictable mechanical performance, and reliable components qualification. In this thesis, the microstructural stability, phase evolution, and mechanical properties of LPBF built 17-4PH SS were systematically investigated as a function of build arrangement, powder feedstock characteristics and laser scan strategies.

Available for download on Thursday, December 31, 2026

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