Structural fatigue in spinel electrodes in high voltage (4 V) Li/Li < inf> x Mn < inf> 2 O < inf> 4 cells

Document Type

Article

Publication Date

1-1-1998

Abstract

Evidence of structural fatigue has been detected at the surface of discharged Lix[Mn2]O4 spinel electrodes in (4 V) Li/Lix[Mn2]O4 cells. Under nonequilibrium conditions, domains of tetragonal Li2[Mn2]O4 coexist with cubic Li[Mn2]O4, even at 500 mV above the thermodynamic voltage expected for the onset of the tetragonal phase. The presence of Li2[Mn2]O4 on the particle surface may contribute to some of the capacity fade observed during cycling of Li/Lix[Mn2]O4 cells. © 1998 The Electrochemical Society, Inc.

Publication Title

Electrochemical and Solid-State Letters

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